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Download Novel Trends in Electroorganic Synthesis by Alessandro Galia, Giuseppe Filardo, Onofrio Scialdone, PDF

By Alessandro Galia, Giuseppe Filardo, Onofrio Scialdone, Massimo Musacco (auth.), Sigeru Torii (eds.)

Among the subjects of curiosity to natural chemists at the present time are the flexibility and area of expertise of electrolysis approaches in natural synthesis, in addition to the most recent advances in method, together with uncomplicated strategies for the layout of electrolysis stipulations and gear. The foreign Symposium on Electroorganic Synthesis met in Kurashiki, Japan, in September 1997 for lectures on all facets of present examine within the box. This quantity comprising the papers from the symposium includes components. half I, Electrooxidation, comprises papers on alcohols and phenols, olefins and aromatics, halogenation, polymers, and electrodes, between others. incorporated partly II, Electroreduction, are papers on carbonyl compounds, halogen-containing compounds, response with EG bases, and steel complexes. the radical traits offered the following should be of particular curiosity to researchers and graduate scholars in electroorganic chemistry and are a beneficial source for all natural chemists.

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Biochem. 1988, 174, 331. (b) I. W. Richardson and C. Anthony, Biochem. J. 1992, 287, 709. (c) T. K. Harris and V. L. Davidson, Biochemistry 1993, 32, 4362. 5. S. ltoh, H. Kawakami, and S. Fukuzumi, Chern. , 1997, 29. 6. S. ltoh, H. Kawakami, and S. Fukuzumi, submitted for publication. NATURAL PRODUCT SYNTHESES USING PHENOLIC OXIDATION IN THE KEY STEP Shosuke YAMAMURA Department of Chemistry, Faculty of Science and Technology, Keio University, Hiyoshi, Yokohama 223, Japan ABSTRACT Some bioactive isodityrosine and related oligopeptides have been successfully synthesized by means of anodic or TTN oxidation of o,o'-dihalogenated phenols.

Anodo~... ,~ 1. Zn,H• I --- =::::,.. Br 1 l(loAJ OH ISODITYROSINE COOH A A __ COOH NH 2 1~1 OH Scheme2. 5 rnl; neutral media: MeOH 25 rnl), LiCl04 as a supporting salt, glassy carbon beaker as an anode, platinum wire as a cathode, undivided cell]. Consequently, the cresol derivatives carrying chlorine and bromine (3a, b, and d) provided the diaryl ethers (type 4), and the ether linkage was specifically introduced at the bromine position in the case of 3d possessing a pair of different halogen atoms.

S. ltoh, H. Kawakami, and S. Fukuzumi, submitted for publication. NATURAL PRODUCT SYNTHESES USING PHENOLIC OXIDATION IN THE KEY STEP Shosuke YAMAMURA Department of Chemistry, Faculty of Science and Technology, Keio University, Hiyoshi, Yokohama 223, Japan ABSTRACT Some bioactive isodityrosine and related oligopeptides have been successfully synthesized by means of anodic or TTN oxidation of o,o'-dihalogenated phenols. Furthermore, electrochemical synthesis of some sesqui- and diterpenes has also been carried out.

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